Quantification of Bacterial Fatty Acids by Extraction and Methylation.

نویسندگان

  • Mark Politz
  • Rebecca Lennen
  • Brian Pfleger
چکیده

This protocol describes two similar methods for the extraction and methylation of fatty acids from bacterial cultures. The acid derivatization protocol (Lennen et al., 2013; Bligh and Dyer, 1959) results in the extraction and methylation of all fatty acids, both free and bound, from a bacterial culture, while the base derivatization protocol (Lennen and Pfleger, 2013) captures only bound (phospholipid, acyl-thioester) species. After extraction into hexane, the lipids may be analyzed by gas chromatography.

برای دانلود رایگان متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Validation of a new procedure to determine plasma fatty acid concentration and isotopic enrichment.

Assessment of free fatty acid (FFA) concentration and isotopic enrichment is useful for studies of FFA kinetics in vivo. A new procedure to recover the major FFA from plasma for concentration and isotopic enrichment measurements is described and validated. The procedure involves extraction of plasma lipids with hexane, methylation with iodomethane (CH(3)I) to form fatty acid methyl esters (FAME...

متن کامل

Comparative of Physico-Chemical Properties of Wheat Germ Oil Extracted with Cold Press and Supercritical CO2 Extraction

In this study, moisture content, free fatty acids, peroxide, iodine value, unsaponifiable matter, saponification value, fatty acid composition and tocopherol contents of wheat germ oil obtained by SC-CO2 extraction and cold press technology were investigated. Moisture, free fatty acid (FFA), peroxide value, iodine value, unsaponifiable matter and saponification value of cold pres...

متن کامل

Effects of salt stress on total lipid values, fatty acid profiles, omega-3, omega-6 and omega-9, in the brown algea Sargassum boveanum on Bushehr coast

Some algae are rich sources of various beneficial lipids and fatty acids. In recent years, several studies have been performed on algae to evaluate the effect of different salinity treatments on the quantity and quality of these lipids. The present study was performed to investigate the effect of different concentrations of sodium chloride on total lipid content, fatty acid profile, and omega-3...

متن کامل

Evaluation of factors affecting on lipid extraction for recovery of fatty acids from Nannochloropsis oculata micro-algae to biodiesel production

Background: This study aimed at determining the appropriate method for dewatering and drying biomass and selecting a suitable organic solvent for lipid extraction. Methods: Nannochloropsis Oculata was cultured in Gillard F/2 medium and after reaching the end of the stationary growth phase, algal biomass was separated from aqueous by centrifuge and dried through three methods: Oven, Air-dried an...

متن کامل

بررسی میزان اسیدهای چرب اشباع و غیراشباع رایج در برخی محصولات غذایی ایران

Background: Cardiovascular diseases are the main cause of mortality in the world. Diets containing saturated fatty acids, industrial trans fatty acids and unsaturated Cis fatty acids, have different effects on blood lipids, insulin resistance, thrombosis and impaired endothelial cell function. Accordingly, this study aims at measuring the amount of fatty acids in some food products that are com...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

عنوان ژورنال:
  • Bio-protocol

دوره 3 21  شماره 

صفحات  -

تاریخ انتشار 2013